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Advanced chemometric methods as Design of Experiments (DoE) and Multivariate Data Analysis (MVDA) enable to look into cost savings besides ensuring process reliability and robustness. DoE is a standard technique to accelerate process development tasks and gain additional process understanding with a least amount of experiments. MVDA techniques are used for scale- and batch-to-batch comparison investigations, and are making inroads into continuous real-time quality control and assurance.